LC-MS Method Validation
Anneli Kruve and Maarja-Liisa Oldekop: Accounting for matrix effect

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Klipi teostus: UTTV 13.01.2016 47059 vaatamist Keemia ja materjaliteadus


Lisainfo veebis: https://moodle.ut.ee/course/search.php?search=LC-MS+Method+Validation

Seotud videod

LC-MS Method Validation
Ivo Leito: Introduction
05.01.16
LC-MS Method Validation
Hanno Evard: Interpreting results in LoD context
05.01.16
LC-MS Method Validation
Anneli Kruve:  Matrix effect
05.01.16
LC-MS Method Validation
Anneli Kruve:  Calculating matrix effect, recovery and process efficiency
05.01.16
LC-MS Method Validation
Maarja-Liisa Oldekop: Introduction to linearity, linear range and sensitivity
05.01.16
LC-MS Method Validation
Maarja-Liisa Oldekop: Linear range, different ranges
05.01.16
LC-MS Method Validation
Koit Herodes :    Intro to selectivity and confirmation. 
Selectivity: RS and alpha
05.01.16
LC-MS Method Validation
Anneli Kruve: Overview of validation
08.01.16
LC-MS Method Validation
Anneli Kruve and Maarja-Liisa Oldekop: 
Reducing matrix effect
08.01.16
LC-MS Method Validation
Maarja-Liisa Oldekop:  Sensitivity
08.01.16
LC-MS Method Validation
Hanno Evard: Intro to LoD
08.01.16
LC-MS Method Validation
Hanno Evard: Instrumental LoD and method LoD
08.01.16
LC-MS Method Validation
Hanno Evard: Different approaches for estimating LoD
08.01.16
LC-MS Method Validation
Koit Herodes: Detector - side selectivity
08.01.16
LC-MS Method Validation
Riin Rebane:Bias components
08.01.16
LC-MS Method Validation
Anneli Kruve: Degree of validation
13.01.16
LC-MS Method Validation
Hanno Evard: CCα and CCβ
13.01.16
LC-MS Method Validation
Maarja-Liisa Oldekop: Evaluating linearity
13.01.16
LC-MS Method Validation
Anneli Kruve: Accuracy, trueness, precision and measurement uncertainty
20.01.16
LC-MS Method Validation
Anneli Kruve: Experimental design
20.01.16
LC-MS Method Validation
Anneli Kruve: Purpose of validation
20.01.16
LC-MS Method Validation
Hanno Evard: Calculating CCα and CCβ
20.01.16
LC-MS Method Validation
Hanno Evard: Interpreting results with CCα and CCβ
20.01.16
LC-MS Method Validation
Hanno Evard: Important aspects of estimating LoD and CCα,  CCβ
20.01.16
LC-MS Method Validation
Maarja-Liisa Oldekop: Evaluation of linearity
20.01.16
LC-MS Method Validation
Riin Rebane: Precision. Repeatability, intermediate precision, reproducibility
20.01.16
LC-MS Method Validation
Riin Rebane: Precision, trueness, accuracy
20.01.16
LC-MS Method Validation
Koit Herodes:: Assesment of selectivity
20.01.16
LC-MS Method Validation
Anneli Kruve: Practical Evaluation of Matrix Effect and Recovery
05.02.16
LC-MS Method Validation
Anneli Kruve: Qualitative evaluation of matrix effect
05.02.16
LC-MS Method Validation
Riin Rebane: Obtaining a reference value
05.02.16
LC-MS Method Validation
Riin Rebane ja Anneli Kruve: Planning precision experiment
05.02.16
LC-MS Method Validation
Maarja-Liisa Oldekop: Carrying out the experiment for linearity evaluation
05.02.16
LC-MS Method Validation
Hanno Evard: Integration
05.02.16
LC-MS Method Validation
Hanno Evard: Introduction to LoQ
03.03.16
LC-MS Method Validation
Koit Herodes: Introduction to identity confirmation.
03.03.16
LC-MS Method Validation
Koit Herodes: LC retention time for identity confirmation.
03.03.16
LC-MS Method Validation
Karin Kipper: Stability introduction
03.03.16
LC-MS Method Validation
Riin Rebane: Practical aspects of precision and trueness: Different guidelines
03.03.16
LC-MS Method Validation
Ivo Leito: Measurement uncertainty estimation approaches
07.03.16
LC-MS Method Validation
Ivo Leito: Accuracy - relations to different concepts
 
07.03.16
LC-MS Method Validation
Karin Kipper: Different types of stability
07.03.16
LC-MS Method Validation
Karin Kipper: Evaluation of stability 
07.03.16
LC-MS Method Validation
Karin Kipper: Examples about unstable analytes
07.03.16
LC-MS Method Validation
Maarja-Liisa Oldekop ja Hanno Evard : Statistical tests for evaluation of linearity
09.03.16
LC-MS Method Validation
Hanno Evard: Different approaches to estimate LoQ
09.03.16
LC-MS Method Validation
Karin Kipper: Overcoming stability issues
09.03.16
LC-MS Method Validation
Karin Kipper: Ruggedness, robustness intro
09.03.16
LC-MS Method Validation
Karin Kipper: Robustness and ruggedness relation to LC-MS method development
09.03.16
LC-MS Method Validation
Koit: Identity confirmation by MS
09.03.16
LC-MS Method Validation
Karin Kipper: Matrix robustness
11.03.16
LC-MS Method Validation
Karin Kipper: Different ways to evaluate robustness
11.03.16
LC-MS Method Validation
Riin Rebane: Example for calculating intermediate precision
10.07.16
LC-MS Method Validation
Hanno Evard: Calculating LoD
13.07.16
LC-MS Method Validation
Hanno Evard: Calculating LoQ
13.07.16
LC-MS Method Validation
Riin Rebane: Example for calculating repeatability
20.07.16
LC-MS Method Validation
Riin Rebane: Example for calculating Trueness
10.08.16
LC-MS Method Validation
Anneli Kruve: Calculating Matrix Effect by Signals
04.10.16
LC-MS Method Validation
Riin Rebane: Calculating Matrix Effect by Concentrations
04.10.16
LC-MS Method Validation
Anneli Kruve:Calculating matrix effect based on concentrations Slope
04.10.16
LC-MS Method Validation
Riin Rebane: An example of evaluation of linearity: lack-of-fit test
24.11.16
LC-MS Method Validation
Riin Rebane: An example of evaluation of linearity: visual evaluation and residuals
24.11.16
LC-MS Method Validation
Maarja-Liisa Oldekop: An example of linearity evaluation in VaLChrom validation software
24.11.16
LC-MS Method Validation
Maico Lechner: Design of Experiment. DoE
19.11.21
LC-MS Method Validation
Maico Lechner: One Factor at a Time. OFAT
19.11.21