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    LC-MS Method Validation
    Anneli Kruve and Maarja-Liisa Oldekop: Accounting for matrix effect

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    Klipi teostus: UTTV 13.01.2016 49111 vaatamist Keemia ja materjaliteadus


    Lisainfo veebis: https://moodle.ut.ee/course/search.php?search=LC-MS+Method+Validation

    Seotud videod

    LC-MS Method Validation
    Ivo Leito: Introduction
    05.01.16
    LC-MS Method Validation
    Hanno Evard: Interpreting results in LoD context
    05.01.16
    LC-MS Method Validation
    Anneli Kruve:  Matrix effect
    05.01.16
    LC-MS Method Validation
    Anneli Kruve:  Calculating matrix effect, recovery and process efficiency
    05.01.16
    LC-MS Method Validation
    Maarja-Liisa Oldekop: Introduction to linearity, linear range and sensitivity
    05.01.16
    LC-MS Method Validation
    Maarja-Liisa Oldekop: Linear range, different ranges
    05.01.16
    LC-MS Method Validation
    Koit Herodes :    Intro to selectivity and confirmation. 
    Selectivity: RS and alpha
    05.01.16
    LC-MS Method Validation
    Anneli Kruve: Overview of validation
    08.01.16
    LC-MS Method Validation
    Anneli Kruve and Maarja-Liisa Oldekop: 
    Reducing matrix effect
    08.01.16
    LC-MS Method Validation
    Maarja-Liisa Oldekop:  Sensitivity
    08.01.16
    LC-MS Method Validation
    Hanno Evard: Intro to LoD
    08.01.16
    LC-MS Method Validation
    Hanno Evard: Instrumental LoD and method LoD
    08.01.16
    LC-MS Method Validation
    Hanno Evard: Different approaches for estimating LoD
    08.01.16
    LC-MS Method Validation
    Koit Herodes: Detector - side selectivity
    08.01.16
    LC-MS Method Validation
    Riin Rebane:Bias components
    08.01.16
    LC-MS Method Validation
    Anneli Kruve: Degree of validation
    13.01.16
    LC-MS Method Validation
    Hanno Evard: CCα and CCβ
    13.01.16
    LC-MS Method Validation
    Maarja-Liisa Oldekop: Evaluating linearity
    13.01.16
    LC-MS Method Validation
    Anneli Kruve: Accuracy, trueness, precision and measurement uncertainty
    20.01.16
    LC-MS Method Validation
    Anneli Kruve: Experimental design
    20.01.16
    LC-MS Method Validation
    Anneli Kruve: Purpose of validation
    20.01.16
    LC-MS Method Validation
    Hanno Evard: Calculating CCα and CCβ
    20.01.16
    LC-MS Method Validation
    Hanno Evard: Interpreting results with CCα and CCβ
    20.01.16
    LC-MS Method Validation
    Hanno Evard: Important aspects of estimating LoD and CCα,  CCβ
    20.01.16
    LC-MS Method Validation
    Maarja-Liisa Oldekop: Evaluation of linearity
    20.01.16
    LC-MS Method Validation
    Riin Rebane: Precision. Repeatability, intermediate precision, reproducibility
    20.01.16
    LC-MS Method Validation
    Riin Rebane: Precision, trueness, accuracy
    20.01.16
    LC-MS Method Validation
    Koit Herodes:: Assesment of selectivity
    20.01.16
    LC-MS Method Validation
    Anneli Kruve: Practical Evaluation of Matrix Effect and Recovery
    05.02.16
    LC-MS Method Validation
    Anneli Kruve: Qualitative evaluation of matrix effect
    05.02.16
    LC-MS Method Validation
    Riin Rebane: Obtaining a reference value
    05.02.16
    LC-MS Method Validation
    Riin Rebane ja Anneli Kruve: Planning precision experiment
    05.02.16
    LC-MS Method Validation
    Maarja-Liisa Oldekop: Carrying out the experiment for linearity evaluation
    05.02.16
    LC-MS Method Validation
    Hanno Evard: Integration
    05.02.16
    LC-MS Method Validation
    Hanno Evard: Introduction to LoQ
    03.03.16
    LC-MS Method Validation
    Koit Herodes: Introduction to identity confirmation.
    03.03.16
    LC-MS Method Validation
    Koit Herodes: LC retention time for identity confirmation.
    03.03.16
    LC-MS Method Validation
    Karin Kipper: Stability introduction
    03.03.16
    LC-MS Method Validation
    Riin Rebane: Practical aspects of precision and trueness: Different guidelines
    03.03.16
    LC-MS Method Validation
    Ivo Leito: Measurement uncertainty estimation approaches
    07.03.16
    LC-MS Method Validation
    Ivo Leito: Accuracy - relations to different concepts
     
    07.03.16
    LC-MS Method Validation
    Karin Kipper: Different types of stability
    07.03.16
    LC-MS Method Validation
    Karin Kipper: Evaluation of stability 
    07.03.16
    LC-MS Method Validation
    Karin Kipper: Examples about unstable analytes
    07.03.16
    LC-MS Method Validation
    Maarja-Liisa Oldekop ja Hanno Evard : Statistical tests for evaluation of linearity
    09.03.16
    LC-MS Method Validation
    Hanno Evard: Different approaches to estimate LoQ
    09.03.16
    LC-MS Method Validation
    Karin Kipper: Overcoming stability issues
    09.03.16
    LC-MS Method Validation
    Karin Kipper: Ruggedness, robustness intro
    09.03.16
    LC-MS Method Validation
    Karin Kipper: Robustness and ruggedness relation to LC-MS method development
    09.03.16
    LC-MS Method Validation
    Koit: Identity confirmation by MS
    09.03.16
    LC-MS Method Validation
    Karin Kipper: Matrix robustness
    11.03.16
    LC-MS Method Validation
    Karin Kipper: Different ways to evaluate robustness
    11.03.16
    LC-MS Method Validation
    Riin Rebane: Example for calculating intermediate precision
    10.07.16
    LC-MS Method Validation
    Hanno Evard: Calculating LoD
    13.07.16
    LC-MS Method Validation
    Hanno Evard: Calculating LoQ
    13.07.16
    LC-MS Method Validation
    Riin Rebane: Example for calculating repeatability
    20.07.16
    LC-MS Method Validation
    Riin Rebane: Example for calculating Trueness
    10.08.16
    LC-MS Method Validation
    Anneli Kruve: Calculating Matrix Effect by Signals
    04.10.16
    LC-MS Method Validation
    Riin Rebane: Calculating Matrix Effect by Concentrations
    04.10.16
    LC-MS Method Validation
    Anneli Kruve:Calculating matrix effect based on concentrations Slope
    04.10.16
    LC-MS Method Validation
    Riin Rebane: An example of evaluation of linearity: lack-of-fit test
    24.11.16
    LC-MS Method Validation
    Riin Rebane: An example of evaluation of linearity: visual evaluation and residuals
    24.11.16
    LC-MS Method Validation
    Maarja-Liisa Oldekop: An example of linearity evaluation in VaLChrom validation software
    24.11.16
    LC-MS Method Validation
    Maico Lechner: Design of Experiment. DoE
    19.11.21
    LC-MS Method Validation
    Maico Lechner: One Factor at a Time. OFAT
    19.11.21